Metrology FIB-SEM DualBeam

FEI Quanta 3D FEG DualBeam (FIB-SEM)

A dual-beam FIB-SEM combining a field-emission SEM column with a high-current Ga+ focused ion beam. It supports high-vacuum, low-vacuum, and ESEM imaging alongside site-specific milling, cross-sectioning, and gas-assisted deposition for 2D and 3D materials characterization.

FEI Quanta 3D FEG DualBeam FIB-SEM
SEM Resolution 1.2 nm at 30 kV (SE)
Ion Beam Resolution 7 nm at 30 kV
Vacuum Modes High / Low / ESEM
Ion Source Ga LMIS, 1000 hr life

System Capabilities

The Quanta 3D FEG is a versatile high-resolution DualBeam system pairing a field-emission SEM column with a high-current focused ion beam (FIB) for 2D and 3D material characterization. Three electron imaging modes – high-vacuum, low-vacuum, and ESEM – accommodate conductive, non-conductive, and hydrated specimens without additional preparation, including in-situ study of humidity (up to 100% RH) and temperature (up to 1500 °C) effects.

The high-current Ga+ FIB enables fast material removal, automated cross-sectioning recipes, and site-specific milling, while live SEM imaging during milling allows real-time monitoring of the process. A selection of gas chemistries supports material deposition and enhanced or selective etching for both conductive and non-conductive samples.

Operating Modes

High-Vacuum SEM Imaging

Field-emission electron source for high-resolution secondary electron imaging of conductive samples, with backscattered and STEM detection available as optional upgrades.

Low-Vacuum / ESEM Imaging

Charge-free imaging of non-conductive and hydrated specimens up to 4000 Pa and 100% RH.

FIB Milling & Cross-Sectioning

High-current Ga+ ion beam for fast material removal, site-specific cross-sections, and TEM lamella preparation.

Gas-Assisted Deposition & Etch

Multiple gas chemistries for Pt, W, and C deposition plus selective etch to reduce re-deposition during milling.

Technical Specifications

Electron Source Field-emission gun, 200 V – 30 kV accelerating voltage
Electron Beam Resolution 1.2 nm at 30 kV (SE, high-vacuum); 2.9 nm at 1 kV (SE)
Ion Source Ga liquid-metal ion source (LMIS), 1000-hour guaranteed lifetime
Ion Beam Resolution 7 nm at 30 kV at beam coincident point (5 nm at optimal working distance)
Ion Accelerating Voltage / Probe Current 2 – 30 kV; 1 pA – 65 nA in 15 steps
Chamber Vacuum Modes High-vacuum < 6×10⁻⁴ Pa; low-vacuum 10–130 Pa; ESEM 10–4000 Pa
Motorized Stage 5-axis eucentric goniometer stage; X/Y 50 mm, Z 25 mm, tilt -15° to +75°
Gas Chemistry Up to 5 gas injectors; Pt, W, Au, and SiO2 deposition; enhanced and insulator etch chemistries

Comparison: This System vs Conventional Alternative

A high-level comparison to highlight performance and workflow advantages.

Feature This System Conventional Method
Sample Prep & Imaging Combined FIB milling and SEM imaging in one chamber Separate FIB and SEM systems requiring sample transfer
Cross-Sectioning Site-specific, sub-100 nm precision cross-sections Manual mechanical polishing or sectioning
Non-Conductive Samples Charge-free imaging and milling via low-vacuum/ESEM and charge neutralization Requires conductive coating

Common Applications

TEM Lamella Preparation Site-specific lift-out and thinning for TEM/STEM analysis.
Cross-Sectional Analysis Precision, site-specific cross-sections for subsurface imaging and failure analysis.
3D Serial Sectioning Slice-and-view tomography for 3D reconstruction of microstructures.
Non-Conductive Sample Imaging Low-vacuum/ESEM imaging and charge-neutralized milling of insulating or hydrated specimens.

Accessories

The following accessories expand sample preparation and analysis capabilities for the DualBeam.

Omniprobe Lift-Out System
Omniprobe Lift-Out System
In-situ micromanipulator for TEM lamella lift-out and site-specific sample transfer.
Available
Gas Injection System
Gas Injection System
Multi-chemistry injectors for Pt/W/C deposition and enhanced or selective etching.
Available

Individual accessories may be available for lending, subject to availability.
To inquire about borrowing a specific accessory, please Contact the Lab Manager.